عنوان المقالة: Synthesis and Characterization of 6- (4- Acetylphenyl azo) - 3 - Aminobenzoic Acid Complexes for Some Transition Metals
زينب عبدالرزاق جبارة | Zainab Abdul Razzaq Jabarah | 3209
- نوع النشر
- مقال علمي
- المؤلفون بالعربي
- المؤلفون بالإنجليزي
- Abaas Obaid Hussein, Rana., Zainab., Nibras
- الملخص الانجليزي
- Azo dye 6-(4-acetylphenyl azo)-3-aminobenzoic acid was produced by grouping the diazonium salt from 4- aminoacetophenone for 3-aminobenzoic acid. Geometry of azo - ligand was resolved on origin of elemental analysis, spectroscopic studies such as 1H and 13CNMR, FTIR and UV-Vis. Handling produced azo ligand for transition metal chelates at aquatic ethanol for a 1:2 metal: ligand ratio, as well in perfect pH. The metal chelates have been described by utilizing atomic, absorption flame, elemental analysis, FTIR, and UV-Vis, as well conductivity and magnetic susceptibility mechanism. Nature for produced compounds, have been studied, obeyed mole ratio as well, methods of continuous, variation, Beer's law yielded up a condensation rate (1×10-4 - 3×10-4M). High molar were absorbtivity, were observed for complex solutions. On origin data a tetrahedral geometry were assigned for the produced complexes. Biological activity of the produced compounds was assayed.
- تاريخ النشر
- 15/07/2019
- الناشر
- Journal of Global Pharma Technology
- رقم المجلد
- 3
- رقم العدد
- 11
- ISSN/ISBN
- 0975 -8542
- رابط DOI
- www.jgpt.co.in
- رابط الملف
- تحميل (86 مرات التحميل)
- الكلمات المفتاحية
- Metal chelate, Azo dyes, Complexes, Biological activity