عبدالسلام معتوق هميل, مرعي ميلود العجيلي و حامد البغدادي
المؤلفون بالإنجليزي
Abdsalam. M. A. Hamil, Marei. M. El-ajaily , Hamed.A.A Bogdadi
الملخص الانجليزي
ABSTRACT
Two complexes of 5-[(Z)-1-(2-hydroxyphenyl) ethylidene] amino-1, 2, 3, 4-tetrahydro-1,4-phthalazinedione have
been synthesized by the reaction of luminol and 2-hydroxyacetophenone with Co(II) and Ni(II) ions, and then
some physical techniques were used to investigate the complexes, such as CHN elemental analyses, conductivity
measurements, magnetic moments, infrared and electronic spectra.The CHN elemental analyses data showed the
formation of 1:2 [M: L] ratio. The conductivity measurements exhibited the presence of non-electrolytic nature.
The infrared spectral data revealed the coordination trends of the free compound towards the metal ions. The
electronic spectral results showed the proper transitions of the free compound and its complexes. The geometrical
structures of the complexes were confirmed according to the data which obtained from the electronic spectra.
Also, the antibacterial activity of the free compound and its complexes were screened on some pathogenic
bacteria, and showed the existence of an effect.
تاريخ النشر
03/01/2014
الناشر
INTERNATIONAL JOURNAL OF ADVANCES IN PHARMACY, BIOLOGY AND CHEMISTRY