عنوان المقالة:تحضير والتركيب والدراسات الميكروبيلوجية لايونات المرتبطة مع قواعد شف المشتقة من الاورثو فثيل الديهايد Synthesis, Diagnosis and Microbiological Studies of Mn+2, Co+2 , Ni +2, Cu+2 and Hg+2 Chelates of Two Schiff Bases Derived from OPhathaldehyde
ا.د. لقاء خالد عبد الكريم | lekaa khalid abd al-karem | 21746
نوع النشر
مجلة علمية
المؤلفون بالعربي
لقاء خالد عبد الكريم, رحاب كاظم الشمري و ميسون طارق
المؤلفون بالإنجليزي
L.K. Abdul Karem1, R.K. Rahem 1Al-Shemary & M.T. TAWFIQ
الملخص العربي
A new Schiff base derivative ligands [H4L1] and [H2L2] have been produced by condensed ophathaldehyde with ethylene diamine and [N1, N1’E, N1, N1’E)-N1, N1’-(1, 2-phenylenebis (methan-1-yl1ylidene)) diethane-1, 2-diamine] with 2-benzoyl benzoic acid. Schiff base ligands have been separated and categorized by 1H, 13 C-NMR, (CHN) elemental analysis, UV-visible, mass spectroscopy and FTIR methods. Ten new coordination complexes were prepared and structurally diagnosed: [M(L1)Cl2] and [M2(L2)Cl2] where M(II) = Mn (II), Co(II), Ni(II),Cu(II) and Hg(II). The complexes have been typified by FTIR, UV-visble atomic absorption, molar conductance elemental analysis, and magnetic susceptibility. The details of the ligand (H4L1) compounds are getting an octahedral geometry while the complexes of ligand (H2L2) that are get square planar and tetrahedral geometries. Antimicrobial examinations show good results in the sharing complexes.
الملخص الانجليزي
new Schiff base derivative ligands [H4L1] and [H2L2] have been produced by condensed ophathaldehyde with ethylene diamine and [N1, N1’E, N1, N1’E)-N1, N1’-(1, 2-phenylenebis (methan-1-yl1ylidene)) diethane-1, 2-diamine] with 2-benzoyl benzoic acid. Schiff base ligands have been separated and categorized by 1H, 13 C-NMR, (CHN) elemental analysis, UV-visible, mass spectroscopy and FTIR methods. Ten new coordination complexes were prepared and structurally diagnosed: [M(L1)Cl2] and [M2(L2)Cl2] where M(II) = Mn (II), Co(II), Ni(II),Cu(II) and Hg(II). The complexes have been typified by FTIR, UV-visble atomic absorption, molar conductance elemental analysis, and magnetic susceptibility. The details of the ligand (H4L1) compounds are getting an octahedral geometry while the complexes of ligand (H2L2) that are get square planar and tetrahedral geometries. Antimicrobial examinations show good results in the sharing a
تاريخ النشر
15/07/2018
الناشر
Journal of Global Pharma Technology
رقم المجلد
10
رقم العدد
6
الصفحات
107-116
رابط الملف
تحميل (726 مرات التحميل)
رابط خارجي
http://www.jgpt.co.in/index.php/jgpt/article/view/1056/794
الكلمات المفتاحية
Schiff base, Antimicrobial, Diagnosis, O-phathaldehyde. Zz
رجوع