عنوان المقالة:تحضير و تشخيص طيفي و دراسة الفعالية البيولوجيةلبعض معقدات العناصر الانتقالية مع قاعدة شيف جديدة BDBAI Synthesis, Spectral Characterization and Antimicrobial Activity of Some Transition Metal Complexes with New Schiff Base Ligand (BDABI)
الاستاذ الدكتورة ابتهال كاظم كريم حمزة دوش | Prof. Dr.Ibtihal Kadhim Kareem Hamza dosh | 5096
- نوع النشر
- مجلة علمية
- المؤلفون بالعربي
- ابتهال كاظم كريم و فوزي يحيى وداي و سحر عقيل حسين
- المؤلفون بالإنجليزي
- FAWZI YAHYA WADDAI1 , EBTIHAL KADHUM KAREEM2 and SAHAR AQEEL HUSSAIN3
- الملخص العربي
- تحضير وتشخيص قاعدة شيف مشتقة من الازاتين مع بعض العناصر الانتقالية.
- الملخص الانجليزي
- ABSTRACT A new Schiff base derivative ligand (LI) have been produced by condensed isatin and 2,3-diaminobutane (2:1) molar ratio. The (LI) ligand has been separated and distinguished by 1 H,13C-NMR, (CHN) elemental analysis, UV-visible, mass spectroscopy and Fourier Transform infrared (FTIR) methods. The metal ions, cobalt(II), nickel(II) and copper(II) complexes were synthesized with the ligand. The complexes were typified by, UV-Visible, FTIR, atomic absorption, molar conductance, magnetic susceptibility and elemental analysis (CHN) techniques. Octahedral geometry are suggested for the metal complexes based on the results of physico-chemical and spectral techniques. The TLC for (LI) ligand and complexes demonstrated single spot for each, signifying their compounds purity. All these compounds were determined aligned with two classes of human pathogenic; bacteria Gram positive and Gram negative
- تاريخ النشر
- 18/01/2018
- الناشر
- ORIENTAL JOURNAL OF CHEMISTRY www.orientjchem.org An International Open Free Access, Peer Reviewed Research Journal
- رقم المجلد
- 34
- رقم العدد
- 1
- ISSN/ISBN
- 0970-020 X
- الصفحات
- ١-١٠
- الكلمات المفتاحية
- . Keywords: Synthesis, Characterization, Schiff base, Complexes, Antimicrobial activity.