عنوان المقالة: Synthesis, Spectroscopic Investigation and Biological Activity of 5-[(Z)-1- (2-ydroxyphenyl) ethylidene] amino -1, 2, 3, 4-tetrahydro-1, 4 -phthalazinedione Complexes
أ.د. عبدالسلام معتوق هميل | Prof. Dr. Abdusalam Matoog Hamil | 6279
- نوع النشر
- مجلة علمية
- المؤلفون بالعربي
- عبدالسلام معتوق هميل, مرعي ميلود العجيلي و حامد البغدادي
- المؤلفون بالإنجليزي
- Abdsalam. M. A. Hamil, Marei. M. El-ajaily , Hamed.A.A Bogdadi
- الملخص الانجليزي
- ABSTRACT Two complexes of 5-[(Z)-1-(2-hydroxyphenyl) ethylidene] amino-1, 2, 3, 4-tetrahydro-1,4-phthalazinedione have been synthesized by the reaction of luminol and 2-hydroxyacetophenone with Co(II) and Ni(II) ions, and then some physical techniques were used to investigate the complexes, such as CHN elemental analyses, conductivity measurements, magnetic moments, infrared and electronic spectra.The CHN elemental analyses data showed the formation of 1:2 [M: L] ratio. The conductivity measurements exhibited the presence of non-electrolytic nature. The infrared spectral data revealed the coordination trends of the free compound towards the metal ions. The electronic spectral results showed the proper transitions of the free compound and its complexes. The geometrical structures of the complexes were confirmed according to the data which obtained from the electronic spectra. Also, the antibacterial activity of the free compound and its complexes were screened on some pathogenic bacteria, and showed the existence of an effect.
- تاريخ النشر
- 03/01/2014
- الناشر
- INTERNATIONAL JOURNAL OF ADVANCES IN PHARMACY, BIOLOGY AND CHEMISTRY
- رقم المجلد
- 3
- رقم العدد
- 1
- ISSN/ISBN
- ISSN: 2277 – 4688
- رابط الملف
- تحميل (53 مرات التحميل)
- الكلمات المفتاحية
- KEYWORDS:luminal, 2-hydroxyacetophenone, Complexes, Antibacterial Activity.