عنوان المقالة:التخليق والتشخيص الطيفي لتكوين مشتقات الفينانثيرين ذات الكفاءة الواحدة An Efficient One-Pot Approach for the Formation of Phenanthridine Derivative; Synthesis and Spectral Characterisation
بيداء كريم سلمان | Baidaa K. Al-Rubaye | 10030
- Publication Type
- Journal
- Arabic Authors
- محمد جابر الجبوري, هيرمن بوتكايدر, بيداء كريم الربيعي
- English Authors
- Baidaa K Al-Rubaye, Herman Potgieter and Mohamad J Al-Jeboori
- Abstract
- The preparation of the phenanthridine derivative compound was achieved by adopting an efficient one-pot synthetic approach. The condensation of an ethanolic mixture of benzaldehyde, cyclohexanone and ammonium acetate in a 2:1:1 mole ratio resulted in the formation of the title compound. Analytical and spectroscopic techniques were used to confirm the nature of the new compound. A mechanism for the formation of the phenanthridine moiety that is based on three steps has been suggested
- Abstract
- The preparation of the phenanthridine derivative compound was achieved by adopting an efficient one-pot synthetic approach. The condensation of an ethanolic mixture of benzaldehyde, cyclohexanone and ammonium acetate in a 2:1:1 mole ratio resulted in the formation of the title compound. Analytical and spectroscopic techniques were used to confirm the nature of the new compound. A mechanism for the formation of the phenanthridine moiety that is based on three steps has been suggested
- Publication Date
- 6/8/2017
- Publisher
- Pelagia Research Library
- Volume No
- 8
- Issue No
- 3
- ISSN/ISBN
- 0976-8505
- Pages
- 365-370
- Keywords
- Phenanthridine moiety, One-pot reaction, Mannich reaction, Spectroscopic characterisation