عنوان المقالة:التخليق والتشخيص الطيفي لتكوين مشتقات الفينانثيرين ذات الكفاءة الواحدة An Efficient One-Pot Approach for the Formation of Phenanthridine Derivative; Synthesis and Spectral Characterisation
بيداء كريم سلمان | Baidaa K. Al-Rubaye | 10030
Publication Type
Journal
Arabic Authors
محمد جابر الجبوري, هيرمن بوتكايدر, بيداء كريم الربيعي
English Authors
Baidaa K Al-Rubaye, Herman Potgieter and Mohamad J Al-Jeboori
Abstract
The preparation of the phenanthridine derivative compound was achieved by adopting an efficient one-pot synthetic approach. The condensation of an ethanolic mixture of benzaldehyde, cyclohexanone and ammonium acetate in a 2:1:1 mole ratio resulted in the formation of the title compound. Analytical and spectroscopic techniques were used to confirm the nature of the new compound. A mechanism for the formation of the phenanthridine moiety that is based on three steps has been suggested
Abstract
The preparation of the phenanthridine derivative compound was achieved by adopting an efficient one-pot synthetic approach. The condensation of an ethanolic mixture of benzaldehyde, cyclohexanone and ammonium acetate in a 2:1:1 mole ratio resulted in the formation of the title compound. Analytical and spectroscopic techniques were used to confirm the nature of the new compound. A mechanism for the formation of the phenanthridine moiety that is based on three steps has been suggested
Publication Date
6/8/2017
Publisher
Pelagia Research Library
Volume No
8
Issue No
3
ISSN/ISBN
0976-8505
Pages
365-370
Keywords
Phenanthridine moiety, One-pot reaction, Mannich reaction, Spectroscopic characterisation
رجوع