عنوان المقالة:عزل وتشخيص مشتقات التربنويد من جذور نبات طبي شائع isolation and characterization of terpenoid derivatives from medicinal plant roots by ( TLC ,FCC ) Techniques
علاء جعفر محراث | Alaa J.Mahrath | 6260
Publication Type
Journal
Arabic Authors
علاء جعفر محراث / غافل صيهود حسن/ ايهاب كريم عبيد
English Authors
Alaa J.Mahrath / Gafil S.Hassan /Ehad K.Ebid
Abstract
The present work includes separation and identification of triterpenoids like sterol, betulinic acid or oleanolic acid extracted from Alhagi roots plant by three stages. The first one involved extraction with soxhlet and identification process of the crude extract using thin layer chromatography (TLC) technique that depends on difference in the polarity of solvents of the mobile phase, while the second stage was isolation of the oleanolic derivative by flash column chromatography (FCC). The final stage includes full elucidation of isolated component by spectroscopic analysis as Fourier Transformer Infra Red (FT-IR with KBr disk and ATR mode), 1H-NMR, MS, and Elemental Analysis (C:H:N).
Abstract
تضمنت الدراسة عزل وتشخيص مركبين باستخدام تقنية كروموتغرافيا العمود و الصفائح الرقيقة.
Publication Date
5/5/2015
Publisher
adgurupublications
Volume No
13
Issue No
2
ISSN/ISBN
0972-768X
Pages
983-989
Keywords
Medical plants, Sterols, Flash column chromatography.
رجوع